HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Allyloxycarbonyl)benzoic acid → Allyl 4-[(5,6,7,8-tetrahydro5,5,8,8tetramethyl-2-naphthyimethylthio)carbonyl]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Allyloxycarbonyl)benzoic acid | HCID 18349855 | — |
| Reactant | 5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-naphthylmethanethiol | HCID 21474534 | — |
| Product | Allyl 4-[(5,6,7,8-tetrahydro5,5,8,8tetramethyl-2-naphthyimethylthio)carbonyl]benzoate | HCID 22911616 | — |
Reaction Steps
In a manner similar to Example 4(c), by reaction of 2 g (10 mmol) of 4-(allyloxycarbonyl)benzoic acid with 2.34 g (10 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylmethanethiol, 3.4 g (81%) of the expected allyl ester, melting point 79°-80° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05688817 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-d4931041fc044e15b86f32edc73b26fa |
| Source note | uspto-grants-1997_11 |