HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,5,8,8-Tetramethyl-5,6,7,8-tetrahydronaphthalene-2-carbonyl chloride → HCID 21474531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,5,8,8-Tetramethyl-5,6,7,8-tetrahydronaphthalene-2-carbonyl chloride | HCID 2795466 | — |
| Reactant | HCID 21474497 | HCID 21474497 | — |
| Product | HCID 21474531 | HCID 21474531 | — |
Reaction Steps
In a manner similar to Example 1(d), by reaction of 2.5 g (10 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthoyl chloride with 1.98 g (10 mmol) of allyl 5-hydroxymethyl-2-thiophene carboxylate, 3.7 g (90%) of allyl ester are obtained in the form of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05688817 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-6412c3792eaf44f79e1f6e2246264900 |
| Source note | uspto-grants-1997_11 |