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HRID229465

反应详情

EQUATION

反应方程式

HRID 229465 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)C(=O)CBr
HCID21642

1-Bromopinacolone

C6H11BrO

结构：COc1ccc2c(C(OP(=O)(OC)OC)=C3CCCC3)n[nH]c2c1
HCID68850940

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c(C(OP(=O)(OC)OC)=C3CCCC3)nn(CC(=O)C(C)(C)C)c2c1
HCID68854752

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from cyclopentylidene(6-methoxy-1H-indazol-3-yl)methyl dimethyl phosphate and 1-bromo-3,3-dimethylbutan-2-one using the procedure described in Method I Step C of Example 1 followed by RP-HPLC purification using 30-100% MeCN gradient without TFA. It was obtained as a solid following lyophilization. LC-MS: 3.56 min. (m/Z=325.2, 451.2, 473.1).

WORKUP

后处理

  1. customfollowed by RP-HPLC purification
  2. customIt was obtained as a solid following lyophilization
  3. custom3.56 min. (m/Z=325.2, 451.2, 473.1)