Benzoate → Benzoyl Peroxide

HRID 2294746Notes

Reaction equation

HRID 2294746 reaction equation
[C:1]([O-:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C[CH2:11][CH2:12][CH2:13][CH:14]([CH2:17][CH2:18][CH:19]([O:24]S([O-])(=O)=O)CC(C)C)CC.[Na+].[OH2:30]>C([O-])(=O)CCCCCCCCCCCCCCCCC.[Zn+2].C([O-])(=O)CCCCCCCCCCCCCCCCC>[C:1]([O:9][O:30][C:19](=[O:24])[C:18]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:17]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

5

Reactant 3

HCID 242BenzoateHCID 962Water3×HCID 23665772Sodium Tetradecyl Sulfate

Product 1

HCID 7187Benzoyl Peroxide

Reagents, catalysts & solvents 1

HCID 11178Zinc StearateCatalyst

Procedure

In this Example, the mixer was charged with BPO (BPO 75% in water), benzoate, water, and zinc stearate. A preproduct was formed after about 30 minutes of mixing. Nonionic surfactant (Tergitol XD) was then added to emulsify the oil into the water phase. After about 30 minutes, a smooth, short, uniform paste of the following composition was produced.

Workup

  1. customA preproduct was formed after about 30 minutes
  2. additionof mixing
  3. customa smooth, short, uniform paste of the following composition was produced

Sources & evidence

ORD record
ord-a37517538359479bb5f5ecef03b0e980
Source dataset
uspto-grants-1997_11
Patent number
US05690856

Reaction notes

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