Hydrochloric Acid → HCID 11141895, compound

Participants

Reaction Conditions

Reaction Steps

4.32 g (54.0 mM) of dry pyridine was added to 3.40 g (20.0 mM) of 10-undecene-1-ol, followed by stirring for 10 minutes at 0° C. To the mixture, 3.80 g (20.0 mM) of p-toluenesulfonyl chloride was added, followed by stirring for 4 hours at room temperature. After the reaction, the reaction mixture was acidified with 2M-hydrochloric acid (HCl) and extracted with ether to obtain an extract. The extract was dried with anhydrous sodium sulfate, followed by distilling-off of ether to obtain 6.20 g (19.1 mM) of 10-undecenyl p-toluenesulfonate (Yield: 95.5%).

Provenance & Evidence