Benzenebutanol → HCID 57438255, compound

HRID 229476Notes

Reaction equation

HRID 229476 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][OH:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:12].[NH2:13][CH2:14][C:15](=[O:21])[CH2:16][CH2:17][C:18](O)=[O:19]>>[ClH:12].[NH2:13][CH2:14][C:15](=[O:21])[CH2:16][CH2:17][C:18]([O:11][CH2:10][CH2:9][CH2:8][CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)=[O:19]

Participants

3

Reactant 2

HCID 76889BenzenebutanolHCID 123608Aminolevulinic Acid Hydrochloride

Product 1

HCID 57438255HCID 57438255, compound

Procedure

From 4-phenyl-1-butanol (5.0 g; 33 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol) at 70° C. The reaction was complete after 29 h. The yield was 1.22 g (68%).

Workup

  1. customat 70° C

Sources & evidence

ORD record
ord-a12ef2db78e2415c91ba6ff0d183487f
Source dataset
uspto-grants-2009_07
Patent number
US07563819B1

Reaction notes

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