Benzoic Acid → HCID 178508670, compound

Participants

Reaction Steps

To 10 ml of methanol was added 1.45 g of 1,3-diiminoisoindoline, and the solution was then stirred under reflux to dissolve the 1,3-diiminoisoindoline. Afterward, 1.22 g of benzoic acid was added to this methanol solution, and stirring was further continued for 5 minutes under reflux. After cooling, the resultant precipitate was collected by filtration, and then washed with 5 ml of methanol. After drying, 2.54 g (yield=95%) of a white powder was obtained. The melting point and the values of elemental analysis of the obtained compound were as follows. The infrared absorption spectrum of the compound is shown in FIG. 1.

Provenance & Evidence