Diethylene Glycol Monoethyl Ether → HCID 49796702, compound

HRID 229478Notes

Reaction equation

HRID 229478 reaction equation
[CH2:1]([O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8]O)[CH3:2].[ClH:10].[NH2:11][CH2:12][C:13](=[O:19])[CH2:14][CH2:15][C:16]([OH:18])=[O:17]>>[ClH:10].[NH2:11][CH2:12][C:13](=[O:19])[CH2:14][CH2:15][C:16]([O:18][CH2:2][CH2:1][O:3][CH2:4][CH2:5][O:6][CH2:7][CH3:8])=[O:17]

Participants

3

Reactant 2

HCID 8146Diethylene Glycol Monoethyl EtherHCID 123608Aminolevulinic Acid Hydrochloride

Product 1

HCID 49796702HCID 49796702, compound

Procedure

From diethylene glycol monoethyl ether (5.0 g; 37 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol) at 70° C. The reaction was complete after 4 h. The yield was 0.90 g (53%) of light tan solid.

Workup

  1. customat 70° C

Sources & evidence

ORD record
ord-cf02e2ec57bf4d9689f8348278134d43
Source dataset
uspto-grants-2009_07
Patent number
US07563819B1

Reaction notes

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