HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 131720331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 131720332 | HCID 131720332 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131720331 | HCID 131720331 | 88.9% |
Reaction Steps
XX (0.21 mmol, 100 mg) was dissolved in 2 mL methanol and 2 mL 1N NaOH and after 1 hour the solution was acidified with TFA to pH 3. Purification on reversed phase HPLC gave 85 mg (88%) product. ESI (M+H)+ : Calc. 342.2; Found 342.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05691329 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-96e84adb529247afb212b07fa74ce0a6 |
| Source note | uspto-grants-1997_11 |