HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzyl alcohol → 4-Nitrobenzyl 5-amino-4-oxopentanoate Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzyl alcohol | HCID 69275 | — |
| Reactant | Aminolevulinic Acid Hydrochloride | HCID 123608 | — |
| Product | 4-Nitrobenzyl 5-amino-4-oxopentanoate Hydrochloride | HCID 22253149 | — |
Reaction Steps
From 4-nitrobenzyl alcohol (5.0 g; 33 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol). The reaction was complete after 15 min at 135° C. The yield was 0.95 g (52%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07563819B1 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-a3e7e53ee41242e4af228c2a4c7fb567 |
| Source note | uspto-grants-2009_07 |