HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzylic alcohol → HCID 17989818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzylic alcohol | HCID 68008 | — |
| Reactant | Aminolevulinic Acid Hydrochloride | HCID 123608 | — |
| Product | HCID 17989818 | HCID 17989818 | — |
Reaction Steps
From 3-fluorobenzyl alcohol (5.1 g; 40 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol). The reaction was complete after 20 h at 100° C. The yield was 1.04 g (72%). Mp 115-119° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07563819B1 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-a85e7d51024f40429cc14c3648527dda |
| Source note | uspto-grants-2009_07 |