HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21471618, compound → 1-(Pyrazin-2-yl)ethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21471618 | HCID 21471618 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(Pyrazin-2-yl)ethanamine | HCID 18519006 | 88.1% |
Reaction Steps
2-(1-Azidoethyl)pyrazine (0.77 g) and 10% palladium on carbon (0.075 g) were stirred in ethanol (40 mL) under an atmosphere of hydrogen at room temperature for 2 h. The mixture was filtered through a pad of celite and the filtrate concentrated under reduced pressure to yield 2-(1-aminoethyl)pyrazine (0.56 g) as a pale oil
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05691323 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-171f8a9ca6af4be2be89e473ecc702da |
| Source note | uspto-grants-1997_11 |