Methanesulfonyl chloride → HCID 13857264, compound

Participants

Reaction Steps

To a solution of N-tert-butoxycarbonyl-D-Phenylalaninol (754 mg) and TEA (0.5 ml) in dichloromethane was added methanesulfonyl chloride (0.28 ml) at 0°-5° C. The reaction mixture was stirred at 0°-5° C. for 30 min, quenched with water, and extracted with dichloromethane.

Provenance & Evidence