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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2295280Generated: October 30, 2026

Phenyl chloroformate → HCID 20475073, compound

https://huagongshe.com/reaction/2295280

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenyl chloroformateHCID 15891—
Reactant5,11-Dihydro-6H-pyrido(2,3-b)(1,4)benzodiazepin-6-oneHCID 70169—
SolventTolueneHCID 1140—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 20475073HCID 20475073—

Reaction Steps

From 5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and phenyl chlorocarbonate in a mixture of dioxan and toluene, 5,11-dihydro-11-phenyloxycarbonyl-6H-pyrido[2,3-b][1,4]-benzodiazepin-6-one was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04424222
Source datasetuspto-grants-1984_01
ORD IDord-601fc40d7245471aa3dc599918d52124
Source noteuspto-grants-1984_01