Benzoyl chloride, 3-nitro- → HCID 178479676, compound

HRID 2295345Notes

Reaction equation

HRID 2295345 reaction equation
Cl.[C:2]1([C:8]2[NH:13][C:12]3[CH:14]=[N:15][CH:16]=[CH:17][C:11]=3[NH:10][N:9]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[N+:18]([C:21]1[CH:22]=[C:23]([CH:27]=[CH:28][CH:29]=1)[C:24]([Cl:26])=[O:25])([O-:20])=[O:19]>>[ClH:26].[N+:18]([C:21]1[CH:22]=[C:23]([CH:27]=[CH:28][CH:29]=1)[C:24]([N:10]1[C:11]2[CH:17]=[CH:16][N:15]=[CH:14][C:12]=2[NH:13][C:8]([C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)=[N:9]1)=[O:25])([O-:20])=[O:19]

Participants

3

Reactant 2

HCID 8495Benzoyl chloride, 3-nitro-HCID 178477991HCID 178477991, compound

Product 1

HCID 178479676HCID 178479676, compoundYield 78.6%

Procedure

3.8 g (0.015 moles) of 3-phenyl-1,4-dihydropyrido[3,4-e]-as-triazine hydrochloride are reacted with m-nitrobenzoyl chloride as described in Example 3 to obtain 1-(m-nitrobenzoyl)-3-phenyl-1,4-dihydropyrido[3,4-e]-as-triazine hydrochloride with a yield of 78.6%; m.p.: 206°-207° C.

Sources & evidence

ORD record
ord-f80de10195664cbb92de0872d283508b
Source dataset
uspto-grants-1984_01
Patent number
US04424351

Reaction notes

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