2-Furancarbonyl chloride → HCID 178479678, compound

HRID 2295346Notes

Reaction equation

HRID 2295346 reaction equation
Cl.[C:2]1([C:8]2[NH:13][C:12]3[CH:14]=[N:15][CH:16]=[CH:17][C:11]=3[NH:10][N:9]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[O:18]1[CH:22]=[CH:21][CH:20]=[C:19]1[C:23]([Cl:25])=[O:24]>>[ClH:25].[O:18]1[CH:22]=[CH:21][CH:20]=[C:19]1[C:23]([N:10]1[C:11]2[CH:17]=[CH:16][N:15]=[CH:14][C:12]=2[NH:13][C:8]([C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)=[N:9]1)=[O:24]

Participants

3

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 178477991HCID 178477991, compound

Product 1

HCID 178479678HCID 178479678, compoundYield 81.1%

Procedure

3.8 g (0.015 moles) of 3-phenyl-1,4-dihydropyrido[3,4-e]-as-triazine hydrochloride are reacted with furan-2-carbonyl chloride as described in Example 2 to obtain 1-furoyl-3-phenyl-1,4-dihydropyrido[3,4-e]-as-triazine hydrochloride with a yield of 81.1%; m.p.: 245°-246° C.

Sources & evidence

ORD record
ord-a889a2e169854555a57942328e8eb452
Source dataset
uspto-grants-1984_01
Patent number
US04424351

Reaction notes

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