4-Chlorobenzoyl chloride → HCID 178479675, compound

HRID 2295347Notes

Reaction equation

HRID 2295347 reaction equation
Cl.[C:2]1([C:8]2[NH:13][C:12]3[CH:14]=[N:15][CH:16]=[CH:17][C:11]=3[NH:10][N:9]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Cl:18][C:19]1[CH:27]=[CH:26][C:22]([C:23](Cl)=[O:24])=[CH:21][CH:20]=1>>[ClH:18].[Cl:18][C:19]1[CH:27]=[CH:26][C:22]([C:23]([N:10]2[C:11]3[CH:17]=[CH:16][N:15]=[CH:14][C:12]=3[NH:13][C:8]([C:2]3[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=3)=[N:9]2)=[O:24])=[CH:21][CH:20]=1

Participants

3

Reactant 2

HCID 85014-Chlorobenzoyl chlorideHCID 178477991HCID 178477991, compound

Product 1

HCID 178479675HCID 178479675, compoundYield 68%

Procedure

3.8 g (0.015 moles) of 3-phenyl-1,4-dihydropyrido[3,4-e]-as-triazine hydrochloride are reacted with p-chlorobenzoyl chloride as described in Example 2 to obtain 1-(p-chlorobenzoyl)-3-phenyl-1,4-dihydropyrido[3,4-e]-as-triazine hydrochloride with a yield of 68%; m.p.: 215° C.

Sources & evidence

ORD record
ord-3815256cfc384ced8f6caf99efd48681
Source dataset
uspto-grants-1984_01
Patent number
US04424351

Reaction notes

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