3-Phenylprop-2-enoyl chloride → HCID 70506413, compound

HRID 2295350Notes

Reaction equation

HRID 2295350 reaction equation
Cl.[CH2:2]([C:9]1[NH:10][NH:11][C:12]2[CH:18]=[CH:17][N:16]=[CH:15][C:13]=2[N:14]=1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:19]([Cl:29])(=[O:28])[CH:20]=[CH:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[ClH:29].[CH2:2]([C:9]1[NH:10][N:11]([C:19](=[O:28])[CH:20]=[CH:21][C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[C:12]2[CH:18]=[CH:17][N:16]=[CH:15][C:13]=2[N:14]=1)[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 660233-Phenylprop-2-enoyl chlorideHCID 12340877HCID 12340877, compound

Product 1

HCID 70506413HCID 70506413, compoundYield 78%

Procedure

3-Benzyl-1,2-dihydropyrido[3,4-e]-as-triazine hydrochloride is reacted with cinnamoyl chloride as described in Example 1 to obtain 3-benzyl-1-cinnamoyl-1,2-dihydropyrido[3,4-e]-as-triazine hydrochloride with a yield of 78%; m.p.: 228° C.

Sources & evidence

ORD record
ord-e3a726e6d15e42c08ad2d0971d3054df
Source dataset
uspto-grants-1984_01
Patent number
US04424351

Reaction notes

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