HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → Vinyl benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | Vinyl Acetate | HCID 7904 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Vinyl benzoate | HCID 13037 | — |
Reaction Steps
Analogously to the procedure described in Example I, 0.28 g of the polymer prepared according to Example 15 and having a palladium content of 19.7% by weight are warmed with 12.2 g of benzoic acid and 55.4 ml of vinyl acetate. In the first reaction run, 76% of theory of vinyl benzoate are isolated after 22 hours. In a further reaction batch with the same polymer, 76% of theory of vinyl benzoate are obtained after 20 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04424359 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-c15d04accf3d48cf9d5b861075f7a8fa |
| Source note | uspto-grants-1984_01 |