HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 20282923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86739172 | HCID 86739172 | — |
| Catalyst | Potassium Iodide | HCID 4875 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20282923 | HCID 20282923 | 71% |
Reaction Steps
A mixture of 2,4-dihydroxy-3-propylsalicylaldehyde (15.5 g), benzyl chloride (12.0 g), potassium carbonate (13 g) and potassium iodide (0.5 g) in dry acetone (350 ml) was heated under reflux for 24 hours. The solid was removed by filtration and the solution evaporated to dryness. The oil obtained was distilled and the fraction bp0.5 mm 220°-224° was collected to yield 15.0 g of 4-benzyloxy-3-propylsalicylaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04424231 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-830b6f45588a43b49e8e15cec9c644ef |
| Source note | uspto-grants-1984_01 |