HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mercaptobenzoic Acid → S-(1-isoquinolyl-methyl)-2-mercapto-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mercaptobenzoic Acid | HCID 5443 | — |
| Reactant | 1-(Chloromethyl)isoquinoline | HCID 13221031 | — |
| Product | S-(1-isoquinolyl-methyl)-2-mercapto-benzoic acid | HCID 57295078 | — |
Reaction Steps
Following the procedure described in Example 16 but starting from 1.8 g. of 1-chloromethyl-isoquinoline and 1.54 g. of thiosalicylic acid, 1.1 g. of S-(1-isoquinolyl-methyl)-2-mercapto-benzoic acid are obtained, melting at 170° to 172° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04425349 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-3cd7959fe43f4c8596ee4585ee319dc9 |
| Source note | uspto-grants-1984_01 |