Phenylacetyl chloride → HCID 20474695, compound

HRID 2295506Notes

Reaction equation

HRID 2295506 reaction equation
[C:1]1([CH2:7][C:8](Cl)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:11][C:12](=[N:17][C:18]1[C:23]([CH3:24])=[CH:22][CH:21]=[CH:20][C:19]=1[CH3:25])[C:13]([O:15][CH3:16])=[O:14]>C1(C)C=CC=CC=1>[CH3:24][C:23]1[CH:22]=[CH:21][CH:20]=[C:19]([CH3:25])[C:18]=1[N:17]([C:12]([C:13]([O:15][CH3:16])=[O:14])=[CH2:11])[C:8](=[O:9])[CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 7679Phenylacetyl chlorideHCID 22973868HCID 22973868, compound

Product 1

HCID 20474695HCID 20474695, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

4.35 ml of phenylacetyl-chloride (0.033 mol) were added dropwise and at room temperature to a solution of 6.7 g (0.03 mol) of N-(methyl-methoxycarbonyl-methylene)-2,6-dimethyl aniline (prepared as described in example 12 and pure at 92%) in toluene (100 ml).

Sources & evidence

ORD record
ord-35b32141ff0b45c098ca16b6bc23ff45
Source dataset
uspto-grants-1984_01
Patent number
US04425357

Reaction notes

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