HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexane → Ethyl 2-[(hexyloxy)imino]-3-oxobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexane | HCID 8101 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178472877 | HCID 178472877 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Ethyl 2-[(hexyloxy)imino]-3-oxobutanoate | HCID 53879425 | 99.5% |
Reaction Steps
Ethyl 2-hydroxyimino-3-oxobutyrate (syn isomer, 40 g.), N,N-dimethylformamide (200 ml.), potassium carbonate (52 g.) and n-hexyl bromide (41.4 g.) were treated in a similar manner to that of Example F-(1) to give ethyl 2-n-hexyloxyimino-3-oxobutyrate (syn isomer, 60.7 g.), oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04425341 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-5cce958c01e14e46bb65f4ac0c366afd |
| Source note | uspto-grants-1984_01 |