HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylaniline → HCID 20455830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylaniline | HCID 949 | — |
| Reactant | Acetonitrile, anilino- (8CI) | HCID 76372 | — |
| Reactant | HCID 57169066 | HCID 57169066 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20455830 | HCID 20455830 | — |
Reaction Steps
Into a solution of 13.2 g N-cyanomethylaniline in 150 ml acetonitrile is added 25.57 g chloroformic acid-[3-(tert.-butylcarbonylamino)-phenyl]-ester, then with further stirring 12.1 g N,N dimethylaniline is added dropwise and the mixture heated for an additional 15 minutes to boiling. The mixture is stirred after cooling in 1 l ice water, the substance which separates out is taken up and after drying in vacuum is recrystallized from a little acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04426222 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-01b7582bd57c42589a2ac8b730c3c2a6 |
| Source note | uspto-grants-1984_01 |