HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pinacolone → HCID 54037179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pinacolone | HCID 6416 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 5-Chloro-3-methylpenta-1,3-diene | HCID 53727112 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54037179 | HCID 54037179 | 78.6% |
Reaction Steps
According to the procedure described in Example 7, from 116 g of 1-chloro-3-methyl-2,4-pentadiene and 100 g of 3,3-dimethyl-butan-2-one in the presence of 200 g of powdered potassium hydroxide in 600 ml of toluene there are obtained 141 g of crude 2,2,7-trimethyl-6,8-nonadien-3-one which are subjected to a fractional distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04426321 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-565ebb7cccf44d2eaf3f1d7bafc12686 |
| Source note | uspto-grants-1984_01 |