HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromotoluene → 3-(3-methylphenyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromotoluene | HCID 11560 | — |
| Reactant | 3-Bromopyridine | HCID 12286 | — |
| Reactant | 3-(3-methoxyphenyl)pyridine | HCID 4133193 | — |
| Product | 3-(3-methylphenyl)pyridine | HCID 4133190 | — |
Reaction Steps
3-(3-methylphenyl)-pyridine was prepared from 81.5 g (0.52 mol) 3-bromopyridine and 120 g (0.70 mol) 3-bromotoluene as described for the preparation of 3-(3-methoxyphenyl)-pyridine. (Example I7). B.p. 87°/0.05 mmHg. Yield 61.7 g (69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04426386 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-f9b7ab7602794b9d807a8407d65e8747 |
| Source note | uspto-grants-1984_01 |