HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 86739184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | [2-Methyl-3-(pyridin-2-yl)phenyl]methanol | HCID 13243428 | — |
| Reactant | cis-3-(2-Chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarbonyl chloride | HCID 86737382 | — |
| Reactant | HCID 86739185 | HCID 86739185 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86739184 | HCID 86739184 | — |
Reaction Steps
This reaction was conducted in the manner of Example 3, Step 2 using 0.58 g (0.002 mol) of cis-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarbonyl chloride, 0.44 g (0.002 mol) of 2-methyl-3-(2-pyridyl)phenylmethanol, and 0.18 mL (0.002 mol) of pyridine in 30 mL of toluene. The yield of [2-methyl-3-pyridin-2-yl)phenyl]methyl cis-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarboxylate was 0.8 g, b.p. 170° C./0.05 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04426524 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-c473a9df0ad647a495298cdc326cfefe |
| Source note | uspto-grants-1984_01 |