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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2295866Generated: November 1, 2026

Pyridine → HCID 86739184, compound

https://huagongshe.com/reaction/2295866

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
Reactant[2-Methyl-3-(pyridin-2-yl)phenyl]methanolHCID 13243428—
Reactantcis-3-(2-Chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarbonyl chlorideHCID 86737382—
ReactantHCID 86739185HCID 86739185—
SolventTolueneHCID 1140—
ProductHCID 86739184HCID 86739184—

Reaction Steps

This reaction was conducted in the manner of Example 3, Step 2 using 0.58 g (0.002 mol) of cis-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarbonyl chloride, 0.44 g (0.002 mol) of 2-methyl-3-(2-pyridyl)phenylmethanol, and 0.18 mL (0.002 mol) of pyridine in 30 mL of toluene. The yield of [2-methyl-3-pyridin-2-yl)phenyl]methyl cis-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarboxylate was 0.8 g, b.p. 170° C./0.05 mm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04426524
Source datasetuspto-grants-1984_01
ORD IDord-c473a9df0ad647a495298cdc326cfefe
Source noteuspto-grants-1984_01