HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl iodide → Butanoic acid, 2-[(1-methylethoxy)imino]-3-oxo-, ethyl ester, (Z)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178472877 | HCID 178472877 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Butanoic acid, 2-[(1-methylethoxy)imino]-3-oxo-, ethyl ester, (Z)- | HCID 539498 | 93.3% |
Reaction Steps
Ethyl 2-hydroxyimino-3-oxobutyrate (syn isomer, 30 g.), iso-propyl iodide (32.5 g.), potassium carbonate (39.5 g.) and acetone (150 ml.) were treated in a similar manner to that of Example D-(1) to give ethyl 2-iso-propoxyimino-3-oxobutyrate (syn isomer, 35.4 g.), oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04427674 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-9eeecb041529464b86d096a603bb3ed3 |
| Source note | uspto-grants-1984_01 |