HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → Ethyl 2-(2-chloroethoxyimino)-3-oxo-4-chlorobutyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | Ethyl 2-[(2-chloroethoxy)imino]-3-oxobutanoate | HCID 54193086 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Ethyl 2-(2-chloroethoxyimino)-3-oxo-4-chlorobutyrate | HCID 54169228 | 70.4% |
Reaction Steps
Ethyl 2-(2-chloroethoxyimino)-3-oxobutyrate (syn isomer, 83.6 g.), sulfury chloride (52.4 g.) and acetic acid (83.6 ml.) were treated in a similar manner to that of Example F-(2) to give Ethyl 2-(2-chloroethoxyimino)-3-oxo-4-chlorobutyrate (syn isomer, 68 g.), oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04427674 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-95e601e06a944069a0f643bf1ba6d62e |
| Source note | uspto-grants-1984_01 |