HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2296381Generated: November 1, 2026
Triphenylphosphine → Phosphonium, triphenyl(2-pyridinylmethyl)-, chloride
https://huagongshe.com/reaction/2296381
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Picolyl chloride | HCID 23393 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Phosphonium, triphenyl(2-pyridinylmethyl)-, chloride | HCID 11058219 | — |
Reaction Steps
A mixture of 60 parts by volume of DMF, 6.4 parts of 2-picolyl chloride and 13.2 parts of triphenylphosphine is stirred at 100° C. under nitrogen for 4 hours. The crystals which have precipitated are filtered off with suction, washed with petroleum ether and dried. 12 parts=59% of theory of triphenyl-2-picolylphosphonium chloride are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04429130 |
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| Source dataset | uspto-grants-1984_01 |
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| ORD ID | ord-3c792c6a89194194931680bac5a162b0 |
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| Source note | uspto-grants-1984_01 |
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