HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 69701332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Cuminaldehyde | HCID 326 | — |
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Sorbitol | HCID 5780 | — |
| Product | HCID 69701332 | HCID 69701332 | 93% |
Reaction Steps
The reaction procedure of Example 8 is repeated in the same manner with the exception of using 26.8 g of sorbitol, 48.0 g of p-isopropylbenzaldehyde, 1.0 g of C9 alkylbenzenesulfonic acid, 9 ml of dimethylsulfoxide, 120 ml of benzene and 100 ml of isopropanol. The reaction is conducted in a semisolid phase for 3 hours, giving di-(p-isopropylbenzylidene)sorbitol in a yield of 93% with a purity of 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04429140 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-e48139c41aad40a19a4c4f451c38ff67 |
| Source note | uspto-grants-1984_01 |