HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 178520273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Trichloroethylene | HCID 6575 | — |
| Reactant | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Reactant | HCID 178418489 | HCID 178418489 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178520273 | HCID 178520273 | 92% |
Reaction Steps
A powdery reaction mixture is obtained in the same manner as in Example 8 with the exception of using 24.0 g of xylitol, 41.5 g of p-chlorobenzaldehyde, 0.5 g of 50% sulfuric acid, 60 ml of trichloroethylene and 18 ml of dioxane. The mixture is similarly after-treated, affording di-(p-chlorobenzylidene)xylitol in a yield of 92% with a purity of 97%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04429140 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-c6f1e598aa40410794e06d0835325e87 |
| Source note | uspto-grants-1984_01 |