HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethylcyclohexan-1-amine → 2-Ethylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethylcyclohexan-1-amine | HCID 544854 | — |
| Reactant | Calciumoxide | HCID 6850728 | — |
| Reactant | Alumina | HCID 9989226 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 2-Ethylaniline | HCID 11357 | 95% |
Reaction Steps
The procedure described in Example 27 is followed, using a reaction temperature of 250° C. and a catalyst which contains 0.5% by weight of palladium on a mixture of 19.4% by weight of calcium oxide and 80.6% by weight of aluminum oxide, and starting from 2-ethylcyclohexylamine. o-Ethylaniline (boiling point=210° C.) is obtained in a yield of 95% of the theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04429155 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-7047ce36165548e0b0dda930a92fa923 |
| Source note | uspto-grants-1984_01 |