2,6-Diethylcyclohexan-1-amine → 2,6-Diethylaniline
Reaction equation
[CH2:1]([CH:3]1[CH2:8][CH2:7][CH2:6][CH:5]([CH2:9][CH3:10])[CH:4]1[NH2:11])[CH3:2]>[Pd]>[CH2:1]([C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([CH2:9][CH3:10])[C:4]=1[NH2:11])[CH3:2]Participants
3
Reagents, catalysts & solvents 1
Procedure
The procedure described in Example 27 is followed, using a catalyst which contains 1.0% by weight of palladium on a cobalt/aluminum spinel and starting from 2,6-diethylcyclohexylamine. 2,6-Diethylaniline (boiling point=243° C.) is obtained in a yield of 96% of the theory.
Sources & evidence
- ORD record
- ord-72356d9cb85345efa38924bec0c4de91
- Source dataset
- uspto-grants-1984_01
- Patent number
- US04429155
Reaction notes
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