HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → HCID 131722131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | HCID 178434543 | HCID 178434543 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131722131 | HCID 131722131 | 98% |
Reaction Steps
116 g (1.0 mol) of 4-chloro-3-methylpyrazole were dissolved in 115 g (1.0 mol) of phosphoric acid (85%) at room temperature. The water contained in the phosphoric acid was evaporated. After a few hours, the title compound crystallized out of the oil initially present (yield 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06488734B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-48b74fdb733349b5a3067534f378c7de |
| Source note | uspto-grants-2002_12 |