137521-34-7 → HCID 277954, compound

HRID 2296638Notes

Reaction equation

HRID 2296638 reaction equation
[CH2:1]([CH:4]1[NH:9][C:8](=[O:10])[CH2:7][CH2:6][CH2:5]1)[CH:2]=[CH2:3]>[Pd].CO>[CH2:1]([CH:4]1[NH:9][C:8](=[O:10])[CH2:7][CH2:6][CH2:5]1)[CH2:2][CH3:3]

Participants

4

Reactant 1

HCID 14507689137521-34-7

Product 1

HCID 277954HCID 277954, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

The 6-allyl-piperidine-2-one product of Example 30c is reduced with palladium on carbon in methanol under hydrogen to give the 6-n-propyl-piperidine-2-one.

Sources & evidence

ORD record
ord-ef7b365082a3436994c5ce7fe563376d
Source dataset
uspto-grants-2002_12
Patent number
US06489323B1

Reaction notes

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