HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 10159178, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 22318959 | HCID 22318959 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 10159178 | HCID 10159178 | — |
Reaction Steps
To 56 mg of 3-(2-cyanophenyl)-5-(2-pyridyl)-1-(3-hydroxyphenyl)-1,2-dihydropyridin-2-one were added 1 ml of acetic anhydride and 1 ml of pyridine and the mixture was stirred at room temperature for one night. The reaction solution was concentrated in vacuo and purified by an NH silica gel chromatography (hexane-ethyl acetate system) to give 30 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07563811B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-ed5f4f0549a8414584bebea1f13ab827 |
| Source note | uspto-grants-2009_07 |