HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-2-phenylethene-1-sulfonyl chloride → HCID 22901518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-2-phenylethene-1-sulfonyl chloride | HCID 5369377 | — |
| Reactant | HCID 86587512 | HCID 86587512 | — |
| Product | HCID 22901518 | HCID 22901518 | 66.1% |
Reaction Steps
(2R)-4-Methanesulfonyl-N-(2-tetrahydropyranyloxy)-2-piperazinecarboxamide (266 mg) and trans-β-styrenesulfonyl chloride (210 mg) were used to give 271 mg of (2R)-4-methanesulfonyl-1-(2-phenyl-2-trans-ethenylsulfonyl)-N-(2-tetrahydropyranyloxy)-2-piperazinecarboxamide as amorphous powder in substantially the same manner as in Example 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489324B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-1cb94170b1804ab29af47bc388b37703 |
| Source note | uspto-grants-2002_12 |