HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 22742433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3,4-Dimethyl-10-(3-phthalimidopropyl)-9-acridone | HCID 22742447 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22742433 | HCID 22742433 | — |
Reaction Steps
A mixture of 1.0 g of 3,4-dimethyl-10-(3-phthalimidopropyl)-9-acridone with 340 ml of oxalyl chloride was stirred at room temperature in 100 ml of dichloromethane for 30 min. After evaporating the excessive oxalyl chloride and dichloromethane under reduced pressure, 1.1 g of the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489336B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-7a3d397720204f41a4d54f1c2934b094 |
| Source note | uspto-grants-2002_12 |