Azobisisobutyronitrile → HCID 86583983, compound

Participants

Reaction Conditions

Reaction Steps

To a 500 ml round-bottom flask was added 0.3 mole of 9-anthracenemethylacrylate, 0.5 mole of 3-hydroxypropylacrylate, 0.2 mole of methylmethacrylate, 300 g of THF, and 0.1-3 g of AIBN. The resulting solution was stirred at 60-75° C. for 5-20 hours under nitrogen atmosphere. The reaction mixture was precipitated in ethyl ether or n-hexane. The precipitate was filtered and dried to provide poly[9-anthracenemethylacrylate/3-hydroxypropylacrylate/methylmethacrylate] copolymer of Formula 20. Yield: 82%.

Provenance & Evidence