HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2296888Generated: November 2, 2026
Azobisisobutyronitrile → HCID 86583984, compound
https://huagongshe.com/reaction/2296888
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | 4-Hydroxybutyl acrylate | HCID 75588 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86583984 | HCID 86583984 | 80% |
Reaction Steps
To a 500 ml round-bottom flask was added 0.3 mole of 9-anthracenemethylmethacrylate, 0.5 mole of 4-hydroxybutylacrylate, 0.2 mole of methylmethacrylate, 300 g of THF, and 0.1-3 g of AIBN. The resulting solution was stirred at 60-75° C. for 5-20 hours under nitrogen atmosphere. The reaction mixture was precipitated in ethyl ether or n-hexane. The precipitate was filtered and dried to provide poly[9-anthracenemethylmethacrylate/4-hydroxybutylacrylate/methylmethacrylate] copolymer of Formula 24. Yield: 80%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06489432B2 |
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| Source dataset | uspto-grants-2002_12 |
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| ORD ID | ord-011408af48a0490eb202df1aba015a77 |
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| Source note | uspto-grants-2002_12 |
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