HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15486117, compound → HCID 15486118, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15486117 | HCID 15486117 | — |
| Catalyst | Lindlars catalyst | HCID 131709914 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 15486118 | HCID 15486118 | 99.5% |
Reaction Steps
2 g of 2-(benzotriazole-2-yl)-4-(1,1,3,3-tetramethylbutyl)-6-(1-hexen-3-yl)-phenol and a trace of “Lindlar catalyst” (Fluka) in 25 ml of hexane was hydrogenated for 5 hours under normal hydrogen pressure. Then the reaction mixture was filtered and concentrated to yield 2 g of 2-(benzotriazole-2-yl)-4-(1,1,3,3-tetramethylbutyl)-6-(3-hexyl)-phenol as an orange liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489486B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-d1bde9b7b8e742769f34cb627987ced5 |
| Source note | uspto-grants-2002_12 |