Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2,2'-Bipyridine | HCID 1474 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2,2'-Bipyridine, 1-oxide | HCID 36463 | — |
Reaction Steps
A solution of 2,2′-bipyridyl (1 mmole) in dichloromethane was treated with m-chloroperoxybenzoic acid (2 mmole) at 0° C., and the reaction mixture was stirred at 25° C. for 2 h. Extraction and chromatography gave 2,2′-bipyridyl-N-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06489476B1 |
|---|
| Source dataset | uspto-grants-2002_12 |
|---|
| ORD ID | ord-43a4891415384ffdb49a345a1c50e666 |
|---|
| Source note | uspto-grants-2002_12 |
|---|
