HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2297005Generated: October 29, 2026
Benzoyl Peroxide → 2-(Bromomethyl)-4,6-dimethylpyridine
https://huagongshe.com/reaction/2297005
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | 2,4,6-Trimethylpyridine | HCID 7953 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 2-(Bromomethyl)-4,6-dimethylpyridine | HCID 22280405 | — |
Reaction Steps
A solution of 2,4,6-collidine (1 mmole) in carbon tetrachloride was treated with NBS (5 mmole) and dibenzoyl peroxide (0.25 mmole) at 80° C. for 12 h. The reaction mixture was cooled to 0° C. and the precipitate was filtered. The filtrate was concentrated under vacuum. Chromatography gave 2-bromomethyl-4,6-dimethylpyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06489476B1 |
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| Source dataset | uspto-grants-2002_12 |
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| ORD ID | ord-8125e7f9e4aa455ba181a56dfcb02b18 |
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| Source note | uspto-grants-2002_12 |
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