HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → 5-Diethylphosphono-2-furaldehyde oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Diethyl (5-formylfuran-2-yl)phosphonate | HCID 46784019 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-Diethylphosphono-2-furaldehyde oxime | HCID 86586426 | — |
Reaction Steps
A solution of 5-diethylphosphono-2-furaldehyde (1 mmole) in ethanol was treated with hydroxylamine (1.1 mmole) and sodium acetate (2.2 mmole) at 25° C. for 12 h. Extraction and chromatography gave 5-diethylphosphono-2-furaldehyde oxime.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489476B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-b7621f5abcfd4a698bb94f5f29c14809 |
| Source note | uspto-grants-2002_12 |