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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 229704Generated: October 30, 2026

HCID 22319133, compound → (6-Methoxypyridin-3-yl)(pyridin-2-yl)methanone

https://huagongshe.com/reaction/229704

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22319133HCID 22319133—
CatalystHCID 178418406HCID 178418406—
SolventAcetoneHCID 180—
Product(6-Methoxypyridin-3-yl)(pyridin-2-yl)methanoneHCID 2231907197.3%

Reaction Steps

To a solution of 0.83 g of α-(2-methoxypyridin-5-yl)-2-pyridinemethanol in 20 ml of an acetone was added 1.70 g of activated manganese dioxide, followed by vigorously stirring at room temperature for 30 minutes. The resulting precipitates were filtered off and washed with acetone. Then, the filtrate was concentrated, to give 0.80 g of the title compound as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07563811B2
Source datasetuspto-grants-2009_07
ORD IDord-32be53f2a8794e15bf19412e2eb371c4
Source noteuspto-grants-2009_07