Dinitrofluorobenzene → N-2-methylallyl-N-ethyl-2,4-dinitrobenzeneamine

HRID 2297339Notes

Reaction equation

[CH3:1][C:2](=[CH2:7])[CH2:3][NH:4][CH2:5][CH3:6].[N+:8]([C:11]1[CH:16]=[C:15]([N+:17]([O-:19])=[O:18])[CH:14]=[CH:13][C:12]=1F)([O-:10])=[O:9]>>[CH3:7][C:2](=[CH2:1])[CH2:3][N:4]([CH2:5][CH3:6])[C:12]1[CH:13]=[CH:14][C:15]([N+:17]([O-:19])=[O:18])=[CH:16][C:11]=1[N+:8]([O-:10])=[O:9]

Participants

Reactant 2

HCID 6264Dinitrofluorobenzene

HCID 875872-Propen-1-amine, N-ethyl-2-methyl-

Product 1

HCID 22251445N-2-methylallyl-N-ethyl-2,4-dinitrobenzeneamine

Procedure

Treatment of N-2-methylallyl-N-ethylamine with 2,4-dinitrofluorobenzene as described in Example 1 gave N-2-methylallyl-N-ethyl-2,4-dinitrobenzeneamine as a red oil (13.0 g).

Sources & evidence

ORD record: ord-c6b8776940ab49bb88af536886c2c54f
Source dataset: uspto-grants-2002_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06491988B1

Reaction notes

Loading…