HRID2297394

反应详情

EQUATION

反应方程式

HRID 2297394 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

200 mg of tert-butyl (2S)-2-benzyloxycarbonylamino-3-(4-(3-(4,5-dihydro-1H-imidazol-2-ylcarbamoyl)-propoxy)phenyl)propionate were dissolved in 5 ml of trifluoroacetic acid/water (95/5) and the solution was stirred at room temperature for 15 min. The reaction solution was then concentrated in vacuo. The residue was dissolved in water and the solution was freeze-dried. Yield: 100%.

WORKUP

后处理

  1. concentrationThe reaction solution was then concentrated in vacuo
  2. dissolutionThe residue was dissolved in water
  3. customthe solution was freeze-dried