HRID2297394
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
200 mg of tert-butyl (2S)-2-benzyloxycarbonylamino-3-(4-(3-(4,5-dihydro-1H-imidazol-2-ylcarbamoyl)-propoxy)phenyl)propionate were dissolved in 5 ml of trifluoroacetic acid/water (95/5) and the solution was stirred at room temperature for 15 min. The reaction solution was then concentrated in vacuo. The residue was dissolved in water and the solution was freeze-dried. Yield: 100%.
WORKUP
后处理
- concentrationThe reaction solution was then concentrated in vacuo
- dissolutionThe residue was dissolved in water
- customthe solution was freeze-dried