HCID 18381945, compound → HCID 18381929, compound

Participants

Reaction Steps

1-(3-nitrophenyl)-4-(diphenylmethyl)piperidine (854 mg) was dissolved in ethanol (60 ml), and 10% palladium/carbon (76 mg) was added thereto, followed by stirring the mixture overnight under hydrogen atmosphere. Palladium/carbon was removed by filtration through Celite and the filtrate was concentrated, followed by purifying the residue by silica gel column chromatography (hexane:ethyl acetate=5:4) to obtain 711 mg of 3-(4-(diphenylmethyl)piperidyl)phenylamine. Yield: 90%.

Provenance & Evidence