Methyl iodide → HCID 12237072, compound

HRID 2297608Notes

Reaction equation

HRID 2297608 reaction equation
[CH3:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH2:5][CH2:4][N:3]=1.[I:12][CH3:13]>CC(C)=O>[I-:12].[CH3:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH2:5][CH2:4][N+:3]=1[CH3:13]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 2315021-Methyl-3,4-dihydroisoquinoline

Product 1

HCID 12237072HCID 12237072, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

1-Methyl-3,4-dihydroisoquinoline (780 mg) was dissolved in acetone (7 ml) and iodomethane (0.38 ml) added. The solution was allowed to stand overnight at room temperature. The product was obtained as pale yellow crystals (1.4 g).

Sources & evidence

ORD record
ord-818d695750fd48489a207ea31713dae7
Source dataset
uspto-grants-2002_12
Patent number
US06492378B1

Reaction notes

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